Part Ⅰ Preliminary Exploration of Materials Science and Engineering Chapter 1 Practice for Materials Science and Engineering Experiment 1 Practice for Optical Metallography-Preparation and Observation of Metallographic Sample Experiment 2 Practice for Material Processing-3D Printing Experiment 3 Practice for Energy Materials and Devices-Preparation of Proton Exchange Membrane Fuel Cell Experiment 4 Practice for Electronic Materials and Devices-Preparation and Characterization of Organic Photodetector Experiment 5 Practice for Biomaterials-Observation of Biological Samples Experiment 5.1 Preparation and Observation of Biological Samples by Scanning Electron Microscope Experiment 5.2 Observation of Biological Samples by Fluorescence Microscope Extended Readings Part Ⅱ Fundamentals of Chemistry and Crystallography Chapter 2 Fundamentals of Physical Chemistry Experiment 6 Determination of Combustion Heat Experiment 7 Determination of Saturated Vapor Pressure of Pure Liquid Experiment 8 Construction of Binary Gas-Liquid Phase Diagram Experiment 9 Determination of Rate Constant for Hydrolysis Conversion of Sucrose Experiment 10 Determination of Electromotive Force of Galvanic Cells Experiment 11 Determination of Surface Tension of Ethanol-Water Solutions Experiment 12 Determination of Relative Molecular Weight of Polymer by Viscosity Method Experiment 13 Determination of Crosslink Density of Rubbers by Swelling Method Extended Readings Chapter 3 Fundamentals of Organic Chemistry Experiment 14 Isolation of Alcohol from Red Wine by Simple Distillation Experiment 15 Purification of Naphthalene by Recrystallization Experiment 16 Separation of Liquid Mixture by Liquid-Liquid Extraction Experiment 17 Extraction of Oil from Sunflower Seeds by Solid-Liquid Extraction Experiment 18 Separation of Pigments from Spinach Leaves by Thin Layer Chromatography and Column Chromatography Extended Readings Chapter 4 Fundamentals of Crystallography Experiment 19 Ball Models of Atomic Arrangements in Pure Metal Crystals Experiment 20 Construction and Analysis of Crystal Structure Models Extended Readings Part Ⅲ Material Properties Chapter 5 Mechanical Properties of Materials Experiment 21 Tensile Test of Materials Experiment 21.1 Tensile Properties of Metals and Work Hardening Experiment 21.2 Precise Measurement of Tensile Properties Experiment 21.3 Influence of Molecular Structure and Strain Rate on the Tensile Properties of Polymers Experiment 22 Hardness Test of Materials Experiment 22.1 Heat Treatment and Hardness Test of Metals Experiment 22.2 Shore Hardness Test of Polymers Experiment 23 Charpy Impact Test of Polymers Experiment 24 Compression Test of Materials Experiment 25 Three-Point Bending Test of Materials Experiment 26 Torsion Test of Metals Extended Readings Chapter 6 Physical Properties of Materials Experiment 27 Determination of Ionization Rate of Plasma in Direct Current Sputtering Experiment 28 Coprecipitation Synthesis and Magnetic Properties of Magnetite Nanoparticles Experiment 28.1 Synthesis of Magnetite Nanoparticles by Coprecipitation Method Experiment 28.2 Characterization of Structure and Magnetic Properties of Magnetite Nanoparticles Experiment 29 Nanoemulsion Synthesis and Optical Properties of Iron-Gold Nanocrystals Experiment 30 Preparation of ZnO Thin Film by Sol-Gel Method and Determination of Energy Bandgap Experiment 31 Preparation and Characterization of BaTiO3 Based Piezoelectric Ceramics Extended Readings Part Ⅳ Material Preparation and Treatment Chapter 7 Forming and Heat Treatment Experiment 32 Microstructure Observation of Crystallization and Aluminum Alloy Ingots Experiment 33 Preparation of Stainless Steel Pellets by Powder Metallurgy Method Experiment 34 Construction of Sn-Bi and Sn-Zn Binary Phase Diagrams Experiment 35 Microstructures and Diffusion of Iron-Carbon Alloys Experiment 35.1 Observation of Equilibrium and Non-Equilibrium Microstructures of Iron-Carbon Alloys Experiment 35.2 Surface Carburizing Heat Treatment of Low Carbon Steel Experiment 36 Heat Treatment of Aluminum Alloy for Precipitation Hardening Experiment 37 Forming Process of Polymers and Application in 3D Printing Experiment 37.1 Determination of Melt Flow Index of Thermoplastics Experiment 37.2 Extrusion and Injection Molding of Polymers Experiment 37.3 3D Modeling, Printing, and Tensile Properties Extended Readings Chapter 8 Organic and Polymeric Materials Experiment 38 Preparation of Copolymer with LCST Phase Transition by Atom Transfer Radical Polymerization Experiment 39 Synthesis of Aspirin by Esterification Reaction Experiment 40 Synthesis of Polystyrene Microspheres by Dispersion Polymerization Experiment 41 Synthesis of Organic Semiconductor and Determination of Frontier Orbital Energies Experiment 41.1 Synthesis of Organic Semiconductor Experiment 41.2 Determination of Frontier Orbital Energies by Cyclic Voltammetry Extended Readings Chapter 9 Nanomaterials Experiment 42 Synthesis of Metal Nanoparticles Experiment 42.1 Citrate Synthesis of Gold Nanoparticles Experiment 42.2 Synthesis of Silver Nanoparticles by Chemical Reduction Method Experiment 42.3 Synthesis and Characterization of Au@Ag Core-Shell Composite Nanoparticles Experiment 43 Synthesis of Cadmium Sulfide Nanoparticles by Microemulsion Method Experiment 44 Preparation of Nickel Nanowires by Template Electrodeposition Experiment 45 Synthesis and Characterization of Rod-like Silica Nanoparticles Experiment 46 Preparation of Surface Conductive Glass by Spray Pyrolysis Method Experiment 47 Preparation and Characterization of Porous Thin Films Extended Readings Part Ⅴ Material Applications Chapter 10 Energy Materials Experiment 48 Fabrication and Characterization of Lithium-Ion Batteries Experiment 48.1 Synthesis and Characterization of Cathode Material LiCoO2 Experiment 48.2 Fabrication and Performance Test of Lithium-Ion Batteries Experiment 49 Fabrication and Characterization of Polymer Solar Cell Extended Readings Chapter 11 Electronic Materials and Devices Experiment 50 Magnetron Sputtering Deposition of ITO Thin Film and Hall Effect Test Experiment 51 Fabrication and Characterization of In-Ga-Zn-O Thin Film Transistor Experiment 52 Micro-nano Processing by Lithography Experiment 52.1 Preparation of a Logo Pattern by Photolithography Experiment 52.2 Fabrication of DVD Microstructure and a Simple Microfluidic Device by Soft Lithography Experiment 52.3 Pattern Transfer by Nanoimprint Lithography Experiment 53 Fabrication of Enzyme-Based Glucose Biosensor Extended Readings Chapter 12 Biomaterials Experiment 54 Preparation and Antibacterial Property of Silver-Loaded Activated Carbon Composites Experiment 54.1 Preparation and Structure Characterization of Antibacterial Silver-loaded Activated Carbon Composites Experiment 54.2 Antibacterial Test of Silver-Loaded Activated Carbon Composites Experiment 55 Preparation and In Vitro Cytotoxicity of Pluronic F127-Encapsulated Curcumin Micelles Experiment 55.1 Preparation and Characterization of Pluronic F127-Encapsulated Curcumin Micelles Experiment 55.2 In Vitro Cytotoxicity of Pluronic F127-Encapsulated Curcumin Micelles Experiment 56 Preparation and Bioactivity of Polylactic Acid/Nano- Hydroxyapatite Composite Experiment 56.1 Preparation and Characterization of Polylactic Acid/Nano-Hydroxyapatite Composite Experiment 56.2 Bioactivity Evaluation of Polylactic Acid/Nano-Hydroxyapatite Composite Extended Readings Chapter 13 Materials and Environment Experiment 57 Passivation and Corrosion Behavior of Ferrous Alloys Experiment 58 Salt Spray Test of Metals Experiment 59 Synthesis and Photocatalytic Activity of TiO2 Powder Extended Readings Appendices A1 Experimental Safety A2 Experimental Errors A3 Data Presentation A4 Experimental Report Extended Readings Index
