大学化学实验(College Chemistry Experiments)(胡宝山)(英文版)

《大学化学实验》（英文版）在介绍实验安全规则、常规实验设备及其基本操作的基础上，聚焦化学热力学实验、化学动力学实验、电化学实验、分析测试实验、综合实验、研究型实验等六个大学化学实验涵盖的典型模块，精选了22 个实验。每个实验包含原理简介、实验设备和试剂、实验内容和操作步骤、实验结果记录与分析、注意事项、问题与讨论等部分。本书紧扣理论教学内容知识重点，紧密衔接化学基础知识和实践知识，实验项目代表性强，既可锻炼学生的基本操作能力，也可加深理论与实践之间的联系。 《大学化学实验》（英文版）可作为高等理工院校化学相关专业本科生的教材，可以配套《大学化学》《普通化学》《工科大学化学》等化学类公共基础课程和教材的全英文实验教学要求。

胡宝山，博士/博士后，重庆大学化学化工学院副院长，重庆市引进高层次人才。重庆市新材料研发创新英才。重庆市石墨烯制造业创新中心（重庆市经信委）、重庆市石墨烯产业技术创新联盟（重庆市经信委）专家委员会成员。 “化工过程强化与反应”国家地方联合工程实验室研究骨干。国家 级精品课程资源共享平台《大学化学》课程主讲教师。参编《大学化学》、《大学化学实验》国家精品资源共享课程系列教材。荣获宝钢教育基金会优秀教师奖、唐立新奖教金、重庆市教学成果奖二等奖（排名四）、重庆大学自然科学一等奖（排名二）等。研究领域为碳纳米材料物理化学、电子器件、能源环境催化等交叉方向。

Chapter 1 General Experimental Rules 1 1.1 Lab Safety Rules 1 1.1.1 Chemicals 1 1.1.2 Instruments . 2 1.1.3 Accident Protocol 2 1.1.4 Safety Treatment of Chemical Wastes . 3 1.1.5 Working Principles of Green Chemistry 4 1.2 Experimental Rules 4 1.2.1 Experimental Requirements . 4 1.2.2 Experimental Rules for Students 5 1.3 Data Analysis Rules 7 1.3.1 Significant Figures . 7 1.3.2 Precision and Accuracy 11 Chapter 2 Common Instruments and Basic Operation 13 2.1 Analytical Balances 13 2.1.1 Electronic Analytical Balance . 13 2.1.2 Photoelectronic Analytical Balance . 14 2.2 Solution Preparation 17 2.2.1 Solution Measurement . 17 2.2.2 Basic Instruments and Operating Methods . 20 2.2.3 Titration Operating . 24 2.3 Preparation and Purification 26 2.3.1 Preparation and Collection of Gases 26 2.3.2 Recrystallization 27 2.4 Analysis and Testing 29 2.4.1 Spectrophotometer . 29 2.4.2 pH Meter 33 2.4.3 Potentiometer Electronic Balance . 35 2.4.4 Conductivity Meter 36 2.4.5 DC Stabilized Power Supply 39 Chapter 3 Basic Experiments 42 3.1 Thermodynamic Experiment 42 3.1.1 Determination of Isobaric Thermal Effect 42 3.1.2 Determination of Ideal Gas Constant . 47 3.1.3 Determination of Ionization Constant . 51 3.1.4 Determination of Solubility Product Constant 55 3.2 Reaction Kinetic Experiment 60 3.2.1 Reaction Rate and Influencing Factors 60 3.2.2 Determination of Reaction Order 64 3.2.3 Conversion Rate of Sucrose to Fructose 68 3.2.4 Influence of Catalyst on Reaction Rate 73 3.3 Electrochemical Experiment 79 3.3.1 Voltaic Cell and Electrode Potential 79 3.3.2 Surface Treatment of Metal Materials . 86 3.3.3 Manufacture of a Printed Circuit Board . 90 3.3.4 Electrochemical Corrosion 93 3.4 Analytical Test Experiment 97 3.4.1 Determination of Nitrogen Oxides 97 3.4.2 Determination of Water Hardness 100 3.4.3 Purification and Content Determination of Cupric Sulfate Crystals 106 3.4.4 Determination of COD in Water (Permanganate Index) 110 Chapter 4 Comprehensive Experiments 115 4.1 Treatment of Chromium-Containing Wastewater 115 4.2 Preparation and Characterization of Ferrous Sulfate Amine 118 4.3 Determination of the Molecular Weight of Glucose(Freezing point reduction method) 121 Chapter 5 Research Experiments 127 5.1 Preparation and Fluorescence Property of Luminescent Materials 127 5.2 Preparation of Single-crystal Material by the Hydrothermal Method 129 5.3 Assembly and Testing of Lithium Ion Batteries 134 REFERENCES 137 APPENDIX 139